Pharmacokinetics
Lectures 3 & 4
- One compartment model
- Simplest
- Works for most drugs
- Model: For IV Bolus
- A is the amount of drug in the compartment at any given time
- C is the concentration of drug in the circulation
- V is the volume of distribution
- A = CV
- Assumptions
- Distribution is instantaneous and the compartment is “well stirred”
- That is that the tissue and plasma concentrations are proportional and reach equilibrium quickly
- IV Bolus lasts less than 5 minutes and is directly into a vein.
- K for first order kinetics
- K = km + ke (urinary and biliary)
- First order process Equations
- Important equations
- Ln (C/C0) = -kt
- C/C0 = e-kt
- C = =C0e-kt
- Log C = log C0 – (k/2.303)t
- Graphical presentations of plasma profiles
- Linear or regular plot
- Gives a negative exponential curve
- Concentration on the y-axis
- Time on the x-axis
- Semi-logarithmic plot
- Straight line (but not with multiple compartments)
- Log C on the y-axis
- Time on the x-axis
- The point where the line reaches the y-axis is log C0
- C0 = the initial concentration at t0
- it is the highest concentration for IV bolus
- it is only a theoretical value
- units are micrograms/ml or mg/L
- k can be determined by the slope of the line
- K = 2.303 x slope
- units are time –1
- AUC
- Units are micrograms x time /volume
- AUC is the total bioavailability of a drug after a given dose
- Can be used to calculate clearance, determine bioavailability and determine bioequivalence
- Determining AUC
- Trapezoidal rule
- AUC = the sum of[(Cn-1 +Cn)(tn-tn-1)/2] + Ctn/k
- Where Ctn is C at infinity
- Below: piece of AUC
- Pharmacokinetic Parameters
- C0 (see above)
- The relationship between k and t1/2
- T1/2 = 0.693/k
- Volume of Distribution
- Also called the apparent Vd
- Vd = Dose/C0 (for IV bolus one compartment model only!!!)
- Vd = CL/k or Dose/(AUC x k)
- A 70kg person has about 3 liters of plasma and 42L of total body water
- Useful parameter and indicator for the relative amount of drug in vascular and extravascular tissues
- more drug in extra vascular tissues when the Vd is more than 42L
- Effected by pathophysiological conditions
- Edemia
- Increases the Vd and decreases C
- age
- Decreases Vd and increases C
- Less lean body mass
- If the Vd is less than or equal to 3 L then the drug shows strong plasma protein binding
- Clearance (CL)
- Units are volume/time
- Measure of drug elimination form body
- Most drugs are cleared by 1st order
- rate is proportional to concentration
- the only thing constant in 1st order
- CLT = CLR + CLH + CLB + …
- Proportionality factor
- if the CL goes down and the Vd goes up then t1/2 goes up too
- the change in t1/2 depends on the magnitude of the change in CL and Vd if they are both changing in the same direction
- CL = elimination rate/ Concentration
- CL = dose/AUC
- Renal clearance:
- CLR = renal excretion rate/C
- CLR = (dDu/dt)/C
- Du = drug in urine unchanged
- = total amount excreted unchanged in urine/ AUC
- Fraction of drug excreted unchanged in urine is Fe
- fe = CLR/CL
- =total amount excreted unchanged in urine/Dose
- =ke/k
- (1-fe)
- the fraction eliminated by non-renal routes
- Estimation of parameters from plasma data
- See example on page 15
- Equations
- slope = (log 2 – log 0.2)/1-10 = -0.111h-1
- k = -2.303k = 0.256 hr-1
- C=C0e-kt = 2.58 mg/L
- t1/2 = 0.983/k = 2.7 hr
- AUC = C0/k = 10.08 mg*hr/L
- CL = Dose/AUC = 5.16 L
- Vd=Cl/k = 20.2 L
- More Examples on page 17
- Equations
- C0 = Dose/V
- log A = log A0 –(k/2.303)t
- MIC (minimum inhibitory concentration)
- Equal to C
- C = C0e-kt
- Log C = log C0 – (k/2.303)t
- Estimation of parameters from urinary excretion data
- Non invasive sampling
- Collected fro an interval
- Less accurate than plasma
- To obtain valid data
- Need significant amount unchanged (high Fe)
- Need specific assay (be able to distinguish parent molecule and metabolite)
- Frequent sampling for good curve description
- To get a complete profile you must sample for up to 5-6 half lives
- Must take into consideration the variation s in pH and volume
- Requires complete bladder emptying
- See table on page 19
- Amount excreted in time interval (Du)= Concentration of unchanged drug in urine (C) x the volume of urine (V)
- Excretion rate = Du/t
- Cumulative amount excreted = Du1 + Du2
- ARE = amount remaining to be excreted
- Rate method:
- Use the excretion rate
- Do a semi-logarithmic plot of the rate or excretion against the midpoint time of urine collection
- K can then be calculated from the slope
- The amount of drug excreted unchanged in the urine accumulates asymptotically toward the limiting value
- see fig B-2
- Du(infinity)/Dose = Fe
- Du/t = excretion rate
- Log(dDu/dt) = log (ke*dose) –k/2.303t
- Y-intercept = ke * dose
- Pros
- not required to determine Du infinity
- can determine ke and k from one diagram and then calculate Fe
- Sigma-minus method
- Ln(Duinfinity – Du) = ln Du infinity –kt
- Where t is the actual time at the end of the collection interval (rather than the midpoint)
- Plot amount remaining to be excreted vs time
- slope still used to determine k
- Pros
- less sensitive to incomplete bladder emptying because Fe = Du infinity/ dose