300 MHz NMR

Day measurements:Night measurements*:Longterm:

1H1H, 13C (1024 scans)only after consultation

13C (256 scans)1H, 13C, DEPT

19F{1H}19F nodec.11B{1H}11B no dec.

 ______31P{1H}31P nodec.

* Hint:1H spectra will be measured with highest priority!

Please note:CLEAN the tube at the outside!

NMR tube:5 mm

length, at least:18 cm

solvent:only deuterated

filling height:4.5 to 5 cm

Sample name:______

(8 digits maximum)(your acronym)(reaction number)

Amount:______mg

Solvent:______

Date: / Name: / Email: /  / Group:
@wwu.de

300 MHz NMR

Day measurements:Night measurements*:Longterm:

1H1H, 13C (1024 scans)only after consultation

13C (256 scans)1H, 13C, DEPT

19F{1H}19F nodec.11B{1H}11B no dec.

 ______31P{1H}31P nodec.

* Hint:1H spectra will be measured with highest priority!

Please note:CLEAN the tube at the outside!

NMR tube:5 mm

length, at least:18 cm

solvent:only deuterated

filling height:4.5 to 5 cm

Sample name:______

(8 digits maximum)(your acronym)(reaction number)

Amount :______mg

Solvent:______

Date: / Name: / Email: /  / Group:
@wwu.de

400 MHz NMR

(Please, only after consultation and after presentation of carbon spectrum)

1D:2D:

1HgCOSY (1H,1H correlation)

13CgHSQC (1J(C,H) correlation)(13C):______- ______ppm

DEPTgHMBC (2,3J(C,H)-correlation)(13C):______- ______ppm

____________

(Hint: If we have the carbon chemical shift range, we can optimize the 2D spectra for highest resolution!)

Formula:

Sample name:______

(8 digits maximum)(your acronym)(reaction number)

Amount :______mg

Solvent:______

Date: / Name: / Email: /  / Group:
@wwu.de

400 MHz NMR

(Please, only after consultation and after presentation of carbon spectrum)

1D:2D:

1HgCOSY (1H,1H correlation)

13CgHSQC (1J(C,H) correlation)(13C):______- ______ppm

DEPTgHMBC (2,3J(C,H)-correlation)(13C):______- ______ppm

____________

(Hint: If we have the carbon chemical shift range, we can optimize the 2D spectra for highest resolution!)

Formula:

Sample name:______

(8 digits maximum)(your acronym)(reaction number)

Amount :______mg

Solvent:______

Date: / Name: / Email: /  / Group:
@wwu.de

500 & 600 MHz NMR –only after consultation!

1D:2D:VT:

1HgCOSYfrom:______°C

13CgHSQC(13C):______- ______ppm to: ______°C

DEPTgHMBC(13C):______- ______ppm

19F19F19F-gCOSY1H{19F}(19F):______ppm

Formula:

31P{1H} / 31P29Si-DEPT______

11B{1H} / 11B29Si-gHMQC______

1D-NOESY1D-TOCSY ______

Sample name:______

(8 digits maximum)(your acronym)(reaction number)

Amount :______mg

Solvent:______

Date: / Name: / Email: /  / Group:
@wwu.de

500 & 600 MHz NMR – only after consultation!

1D:2D:VT:

1HgCOSYfrom:______°C

13CgHSQC(13C):______- ______ppm to: ______°C

DEPTgHMBC(13C):______- ______ppm

19F19F19F-gCOSY1H{19F}(19F):______ppm

Formula:

31P{1H} / 31P29Si-DEPT______

11B{1H} / 11B29Si-gHMQC______

1D-NOESY1D-TOCSY ______

Sample name:______

(8 digits maximum)(your acronym)(reaction number)

Amount :______mg

Solvent:______

Date: / Name: / Email: /  / Group:
@wwu.de

Name: Group:

Solvent:Sample name: ______

Name: Group:

Solvent:Sample name: ______

Name: Group:

Solvent:Sample name: ______

Name: Group:

Solvent:Sample name: ______

Name: Group:

Solvent:Sample name: ______

Name: Group:

Solvent:Sample name: ______

Name: Group:

Solvent:Sample name: ______

Name: Group:

Solvent:Sample name: ______