Supplementary Material
Zwitterionic Polymer-Grafted MicrospheresPrepared by RAFT Polymerization
Hiromi Kitano,a* Ken-ichiTokuwa,aHarukaUeno,aLifu Li,a Yoshiyuki Saruwatarib
aDepartment of Applied Chemistry, Graduate School of Science and Engineering, University of Toyama, Toyama 930-8555, Japan
bR & D Laboratory, Osaka Organic Chemical Industry Ltd., Kashiwara 582-0020, Japan
S1. Effect of NaCl on the-potential and hydrodynamic diameter of MSs.
(a) (b)
Figure S1ζ-Potential and Dhvalues of polymer-modified microspheres at various concentrations of NaCl and 25 oC. (a) PSSNa-MSand (b) PMOETAC-MS. [PSSNa-MS] =0.01 wt% and [PMOETAC-MS] = 0.01 wt%. [NaCl] = 0, 10, 20, 40, 60, 100 and 150 mM.
S2. Effect of NaCl and proteins on relative hydrodynamic diameter of MSs.
(a) (b)
(c) (d)
FigureS2 Relative Dhvalues of PMOETAC-MS and PSSNa-MS in the presence of BSAand lysozyme at 25 oC.PMOETAC-MS (0.01 wt%) in the presence of (a) BSA and (b) lysozyme. PSSNa-MS (0.01 wt%) in the presence of (c) BSA and (d) lysozyme. [NaCl] = 0.10 M. [BSA] = 4.5 mg/mL. [Lysozyme] = 4.5 mg/mL. The Dh values of microspheres were normalized by that without any additives. The symbol, *, denotes the Dh after incubation inthe indicated solution for 1 h.
S3. Refractive index of polymer-graftedmicrospheres.
At first, the surface density of PCMB graft chain (brush) on the PBAmicrosphere(PCMB-MS) was determined. The DP value of PCMB-CTA was determined to be 87 by GPC. The elemental analyses of the PCMB-MS indicated that thePCMB-PBAblock copolymer was composed of 87 residues of CMB and585 residues of BA. Therefore, the molecular weight of PCMB and PBA blocks were 2.1104 and 7.5104, respectively.
The hydrodynamic radius of PCMB-MS was estimated to be 65.5 nm by theDLS measurements. It was previously reported that the length of PCMB brush on the silica micro-particle was 63.6 % of full-stretching[S1]. Taking account of the length of vinyl group (0.254 nm), the length of PCMB brush(DP = 87; full-stretched length, 22.1 nm) in the corona of microspherewas assumed to be 13.9 (= 22.10.636) nm. Consequently, the volume of corona (PCMB brush layer) on theMS (vcorona) was estimated to be 6.0x10-16 mL using equation (S1).
vcorona = (4/3) (r23-r13) (S1)
wherer2 and r1 are the hydrodynamic radii of PCMB-MS (65.5 nm) and PBA core((65.5–13.9 =) 51.6 nm), respectively (Figure S3).
The volume of core composed of PBA (vcore) was given as equation (S2), where X is the number of block copolymer in the microsphere.
(7.5104X)/ NAPBA= (4/3)r13 (S2)
The density of PBA core (PBA) was 1.087 g/cm3, and NA is the Avogadro number. Therefore, X and thegraft density of PCMB were estimated as 5.0103and 0.15 chain/nm2, respectively, and the volume of the core (vcore) was calculated to be 5.810-16mL.
The weight of one microsphere (w) was determined to be 8.010-16 g using equation (S3).
w = (2.1104 + 7.5104)5.0103 / NA (S3)
Since the dispersion was 18.1 weight%, the number of microspheres in 1 mL of thedispersion (N) was determined to be 2.31014.
The volume of PCMB brush in themicrosphere (vPCMB) was estimated to be 1.310-16 mL using equation (S4), where the density of PCMB was assumed to be the same as that of PMPC (1.30 g/cm3)[S2].
vPCMB= 2.1104 5.0103 / (NA 1.30) (S4)
Therefore, the volume of water in the corona (vwater) was given as
vwater = vcorona - vPCMB= 6.010-16– 1.310-16 = 4.710-16mL. (S5)
Consequently, the total volume of microspheres in 1 mL of dispersion (V) was determined as
V = (vcore + vwater + vPCMB) N = 0.28 mL. (S6)
Assuming that the refractive index of the corona (ncorona) is simply the volume-proportional summation of the refractive indices of water and polymer chains (S7), the ncorona value could be determinedto be 1.372.
ncorona = (vwaternwater+ vPCMBnPCMB)/vcorona (S7)
By the similar assumption, the average refractive index of the polymer-modified microsphere (nav) (S8) could be determined to be 1.418.
nav = (nPBAvPBA + ncoronavcorona)/vPCMB-MS (S8)
where the nwater, nPCMB and nPBA values are 1.333, 1.49 (n value for poly(methylmethacrylate))[S3] and 1.466, respectively. The apparent refractive index of the dispersion (np) is given as
np = nav (VPCMB-MS /V) + ns[1- (VPCMB-MS /V)] = nav+ ns (1-) (S9)
whereVand VPCMB-MS denote the total volume of the dispersion and microspheres, respectively, in 1 mL of thedispersion.
The volume fraction of thePCMB-modified MS (VPCMB-MS / V) was 0.28 (S6). Therefore, the np value was approximated to be 1.35.Consequently, the Dobs was estimated as 174 nm using equation (S10), where the peak wavelength (p)was 384 nm (Figure S4).
Dobs = (3/8)0.5 (p/np) (S10)
In a similar manner, the average refractive index (np) of PMA-MS dispersion was estimated to be 1.336 at 4.16 weight%. The peak wavelength (p) was 579 nm (Figure 5 (b) in the text) and,therefore, the Dobs value for thePMA-MS dispersion was determined to be 265 nm using equation (S10).
[S1]Suzuki H, Murou M, Kitano H, Ohno K, Saruwatari Y (2011)ColloidsSurf. B: Biointerfaces 84:111-116.
[S2] Iwata R, Suk-In P, Hoven VP, Takahara A, Akiyoshi K, Iwasaki Y (2004)Biomacromolecules5: 2308-2314.
[S2]Brandrup J, Immergut EH, Grulke EA, Abe A, Bloch D, Polymer Handbook, 4th Edition,Wiley-Interscience, 2003.
Figure S3Image ofvcorona, vcore, vPCMB and vH2O.
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