MOTION OF PARTICLE TROUGH FLUID : FLUIDIZATION

(a)  Fluidization is one of the processes involving the movement of particles through fluid.

(i)  Define ‘ Fluidization ‘

Fluidization is a process whereby agranular materialis converted from a static solid-like state to a dynamicfluid-like state.

(ii)  Describe the purpose of fluidization

The most common reason for fluidizing a bed is to obtain vigorous agitation of the solids in contact with the fluid, leading to an enhanced transport mechanism (diffusion, convection, and mass/energy transfer).

(iii)  Sketch the schematic diagram depicts the fluidization process occurred in the

granular bed column.

(b)  Catalyst pellets 5 mm in diameter are to be fluidized with 45 000 kg/h of water with density 985 kg/m3 at 50 ºC in a vertical cylindrical vessel. The density of the catalyst particles is 1760 kg/m3 and their sphericity is 0.86.

Particle: Pellet

Dp = 5 x 10-3 m

ρp = 1760 kg/m3

Φ = 0.86

Take εM = 0.45

Fluid: Water

m = 45000 kg/h

ρ = 985 kg/m3

µ = 0.6 x 10-3 kg/m.s ( at T=50 ºC)

(i)  Calculate the minimum velocity VOM of the water used to fluidized the catalyst pellets

150μVOMΦS2Dp2 1-εMεM3+1.75ρV2OMΦsDp 1εM3=gρp-ρ

150(0.6 x 10-3)VOM0.8625 x 10-3 2 1-0.450.453+1.75(985)V2OM0.865 x 10-3 10.453=9.811760-985

Solving for VOM VOM=0.0384 m/s

(ii)  Estimate the diameter of the vertical cylindrical vessel

A=mρVOM

A=45000 kghr×1 hr3600s×m3985 kg×s0.0384m

A=0.3305 m2 (Area of cylinder)

A=πD24

0.3305=πD24

D=0.65 m

FLOW OF FLUID THROUGH GRANULAR BEDS

(a)  The specific surface area of particle (S) in one of the parameters affecting the pressure drop of the fluid flows through a granular beds or porous medium. In considering the effect of surface area, there is a difference between the specific surface or particle (S) and the specific surface area of bed (SB). Explain why these two parameters cannot be assumed similar.

S and SB are not equal due to the voidage which is present when the particles are packed into a bed.

(b)  Adsorption process has been conducted in a packed column whereas air was subjected to flow through beds of granular activated carbon at 130 º C under the atmospheric pressure. A pore space which approximately 25% of granular bed form a channel like-tube with diameter of 5.56 x10-4 (L). Based on Carman-Kozeny, the pressure drop per length of the column is given by 1048.48 (Pa/m).

Air properties at T= 130 º C, (interpolation from table appendix A.3.3)

ρ = 0.8768 kg/m3

µ = 2.3020 x 10-5 kg/m.s or Pa.s

ε = 0.25

de = 5.56 x10-4 m

∆pL=1048.48 (Pa/m).

i)  Estimate the average size (Dp (m)) of the activated carbon granule packed in the column.

de=4εSB
5.56 × 10-4=4(0.25)SB

SB=1798.5612

SB=S (1-ε)

1798.5612=S (0.75)

S=2398.0816

S=6DP
2398.0816=6DP

Dp=2.502 ×10-3 m

(c)  Calculate the Reynolds number of the gas flow through the column and state the types of flow occurred in the process.

∆pL=K1-ε2S2ε3μV0

1048.48=50.7522398.081620.253 2.3020 ×10-5 V0

V0=0.044 m/s

Re=ρV0S1-εμ= 0.8768 (0.044)2398.0816 (0.75)( 2.3020 ×10-5 )=0.93

Laminar flow because Re < 1