Department of Chemistry, Dr Harisingh Gour University,

B.Sc. Vth Semester

Industrial Chemistry

(For UTD and College Students Only)

Paper Code / Title / Internal Examination / Main Examination / Internal / Theory
Mains
ICH-501 / Chemistry Process Economics & Management Industries – I / Two CCE Examinations of 10 Marks Each / Final Semester Examinations of 23 Marks Each / (CCE) for 501,502 and 503
BEST OF TWO
10+10+10
Total 30 Marks / 23
Marks
ICH-502 / Assets Recycling -Industrial Organisation &Waste Recycling-I / Two CCE Examinations 10 Marks Each / Final Semester Examinations of 23 Marks Each / 23 Marks
ICH-503 / Waste Recycling- Industrial Chemical Analysis – I / Two CCE Examinations 10 Marks Each / Final Semester Examinations of 24 Marks Each / 24 Marks
CHE-504 / Laboratory Course / NO CCE in Practical / Final Semester Examinations of 50 Marks Each / 50 Marks
Note :
One Project in any one the subjects (Chem, Bot, Zool, Biotech, Mbiol, Phy, Maths etc) of B.Sc. in Consultation with Dean, Academic

INDUSTRIAL CHEMISTRY

B.Sc.- Part-III Semester V

Paper: ICH-501

PAPER-1-Chemistry Process Economics & Management Industries - I

Unit-IFactor involved in project cost estimate Method employed for the estimation of capital investment

Unit-IIDepreciation, method of determining depreciation .Taxes. Some aspects of marketing. Pricing Policy.

Unit-IIIConcept of scientific management in industry. Function of management, decision making, planning, organizing, selecting and control location of industry.

Unit-IVSampling procedures, sampling of bulk materials, Techniques of sampling solids liquids and gases, Collecting and processing of data.

Unit-VUV-visible spectroscopy, IR spectroscopy and non-dispersive IR, Atomic Adsorption. Flame photometry

Industrial Chemistry

B.Sc.- Part-III Semester V

Paper - II- ICH-502

PAPER-II Assets Recycling -Industrial Organisation &Waste Recycling-I

Unit INeed for waste recycle-Conversion of solid waste into useful product

Unit IIIdentification and qualification of industrial, domestic and agro waste. Feasibility of recycle.

Unit IIISolid waste –Removal of solid contaminants from water by coagulation, sedimentation

Unit IVWaste management : Waste water treatment and its reuse in Domestic uses

Unit-VEconomics of recycling of waste

Industrial Chemistry

B.Sc.- Part-III Semester V

Paper – III: ICH - 503

PAPER-III-Waste Recycling- Industrial Chemical Analysis - I

Unit IPhysical and chemical processes used for the recovery of important compounds

Unit II Biology processes for the treatment of waste water

Unit IIIGaseous waste: adsorption, Catalytic conversion

Unit IVCharacterization of waste, their management and recovery of important compounds from the wastes from the following industries.

Unit VSlaughter houses, rubber, sugar, heavy chemicals,

Industrial Chemistry Course

Laboratory Course: ICH-504

B.Sc.- Semester V

PRACTICALS

SECTION-I

Unit I Separation –TLC paper chromatography . V

Unit II Ion Exchange –Ion exchange capacity of Resins. Softening of hard water ,separation of important metal Fe, Ni, Cr , from effluents and their estimation .

Unit IIIActivated - Efficiency of canon adsorption , isotherms ,separation of some important chemicals by adsorption on canon .

Unit IV Fuel pallets from garbage and solids wastes calorific value.

SECTION-II

Unit I The students are expected to collect solid and liquids wastes from nearly industries and analysis with respect to constituent, recovery of important constituent and disposal methods.

Industries Analysis – Analysis of common raw material vas per the industrial specification such as phenol aniline, H2 O2 acetone , epoxide olefine ,oil etc. V

Viva Voce

Industrial Chemistry Vocational Course

B.Sc.- Part-III Semester VI

ICH- 601

PAPER-1-Chemistry Process Economics & Management Industries - II

Unit-ICapital formation .Elements of cost accounting

Interest and investment cost .Time value of money-equivalence

Unit IIProfitability criteria, Economics of selection alternatives.

Variation of cost with capacity .Break even point, optimum batch size, production scheduling etc.

Unit IIIMaterials of industry, Inventory control.

Management of human resources-selection of incentives welfare and safety

Unit-IVChromatography , paper chromatography , TLC, GLC, HPLC

Modern instrument method of analysis

Unit-VIon-selective electrodes, Ion-Chromatography.

NMR-spectroscopy and, Neutron diffraction. X-ray fluorescence

Industrial Chemistry Vocational Course

B.Sc.- Part-III Semester VI

ICH- 602

PAPER-IIAssets Recycling -Industrial Organisation &WasteRecycling-II

Unit IWaste recycle - Limitations of raw material resources. Waste elimination.

Unit IISeparation of Waste - Solid, Liquid and Gaseous.

Unit IIISolid waste disposal, Incineration, Fuel palletization Soil conditioning

Unit IVPhysical & Chemical treatment of water and its reuse in industries viz., Agriculture , Oil refineries , Thermal power station and Reuse of cooling water

Unit-VEconomics of recycling of waste

Industrial Chemistry Vocational Course

B.Sc.- Part-III Semester VI

ICH- 603

PAPER-III-Waste Recycling- Industrial Chemical Analysis - II

Unit IActivation carbon adsorption, Ion exchange process, evaporation, distillation, centrifugation, filtration, coagulation, membrane processes, microbial degradation

Unit IITrickle filters, activated sludge process, microbial degradations.

Unit III Recovery of important gases .CO2, NO2, SO2 etc. electrostatic precipitation bag filter, wetldly grid arrestors

Unit IVDyestuff, fertilizers. Textile. Oil fats and soap and steel plant

Unit VFermentation, thermal power station, electroplating paper paint

Industrial Chemistry Vocational Course

B.Sc.- Part-III Semester VI

ICH- 604

Laboratory Course

SECTION-I

Estimation of SO2, NH3, NO2.

Estimation of hardness acidity and pH of water VI

Estimation of BOD, COD content of effluent water from different industries.

Analysis of solid contents from the liquid effluent form different industries .separation of the constituent, chromatographic.

Synthesis of common industrial compounds involving two step reaction –for examples 4-bromo aniline 3-nitro aniline sulphanilimide +aminobenzoc acid 4-Nitrobenzoic acid Dihalobenzene. Nitrohalobenzene .practical records. VI

Books

1.Science of ceramics Chemical processing, Hench L.L.

2.Chemistry and Physic of Clays other ceramics

3.Science of ceramics, Stewat, G.H.

4.Chemistry of cement

5.Properties of glass Merey, G.W.

6.Chemistry of glasses Paul, G.W.

7.Corrosion Causes and prevention, Spellur, F.N.

8.Corrosion and Corrosion engineering Fontana M.G. and Green N. Dr. McGraw- Hill Book Co.

9.Experiments in materials Technology, a Laboratory Text for Engineers, Manufacturing metallurgy and materials testing Govt. of India East West Publication

10.Selecting Materials for Process Equipment MC Maugton K.J., McGraw Hill Book Co.

11.Industrial instrumentation D.P. Eckpan, John- Wileys & Sons.

12.Applied Instrument in process Industries, Vol. and I & III W.G. Andrens, Gulf Publication

13.Instrumentation and control the process industries S. Borer, Elsevies Applied Science Publishers.

14.Chemical Engineers and book J.H. Terry and D Greenb, McGraw-Hill Publishing Co., New York.

Books

1 / Unit process in Organic Synthesis
P.M. Groggins. McGraw- Hill Book Co., New York
2 / Unit Processes in organic synthesis, P.H. Grroggins, McGraw – Hill Book Ck. New York

Books

1 / Pollution control in chemical and – industries Mahajan S.P.
2 / Pollution control in industries, A series of books by Jones H..R.
3 / System’s Approach to Air pollution Control, R.J. Bibbero and I.G. young.
4 / Air pollution- Vol. I-IV Editor, A.C. stern, Academic Press, New York
5 / Gas purification process for Air pollution control G. Nonhebel Newnes- Butterworth’s, London
6 / Air Pollution Technology. Painter, D.E. Reston Publishing Co-
7 / Effluent Technology in process Industries Inst. of Chems Engg.
8 / Effluent Treatment and waste disposal Inst of Chem Engg
9 / Effluents Treatment and waste disposal Inst. of Chem Engg.
10 / System’s Approach to air pollution control, R.J. Bibbered and I.O. Young.
11 / Air pollution- Vol I, I-IV Editor, A.C. stern, Academic press, New York.
12 / Gas purification process for air pollution control, Nonhebel Newness- Butterworth’s London
13 / Air pollution Technology painter D.E. Reston Publishing Co.