Costs Applicable to Cleanup Procedures
Costs are applicable only when additional cleanup is required beyond that routinely conducted on samples. The costs for cleanups routinely conducted for an analysis are included into the analytical costs.
Task # / Task Description / Matrix / Method / Cost Per Sample1 / Alumina Cleanup / Extract / 3610
2 / Alumina Cleanup / Extract / 3611B
3 / Florisil Cleanup / Extract / 3620
4 / Silica Gel Cleanup / Extract / 3630
5 / Gel Permeation Cleanup / Extract / 3640
6 / Sulfur Cleanup / Extract / 3660
7 / Sulfuric Acid Perm. Cleanup / Extract / 3665
8 / Mercury Cleanup / Extract
Costs for Leaching Procedures to Evaluate the Mobility of Contaminants in Soils
The following costs apply to leaching procedures required when the mobility of contaminants in soils are being evaluated.
Task # / Task Description / Matrix / Method / Cost Per Sample10 / SPLP Bottle Shake Leach / Soil / 1312
11 / SPLP ZHE Leach / Soil / 1312
12 / Neutral ASTM Leach / Soil / D 3987-04
13 / Single ASTM Batch Leach / Soil / D 5233-92
14 / TCLP Bottle Shake Leach / Soil / 1311
15 / TCLP ZHE Leach / Soil / 1311
Metals Analyses
For soils, DEQ Laboratory sample preparation procedure, or equivalent sample preparation procedure, must be used to establish representative soil sub-samples for metals, not including Mercury.
ICPES/ICPMS – Cost Per Sample and Metal
The following costs apply when a customized list of metals is provided to the laboratory for analysis.
Task # / Task Description / Matrix / Preparation / Method / CostPer Metal
20 / Metals - ICP/ES / Water / DEQ Lab / 6010B 200.7
21 / Metals - ICP/ES / Soil / DEQ Lab / 6010B 200.7
22 / Metals - ICP/MS / Water / DEQ Lab / 6020 200.8
23 / Metals - ICP/MS / Soil / DEQ Lab / 6020 200.8
ICPES/ICPMS – Cost Per Sample for a Suite of Metals (full TCL list)
Per Sample
30 / Metals - ICP/ES or ICP/MS / Metals TCL for Waters / Water / ICPES/MS
31 / Metals - ICP/ES or ICP/MS / Metals TCL for Soils / Soil / ICPES/MS
32 / Metals – ICP/ES / Metals TCL for Waters / Water / 6010B 200.7
33 / Metals – ICP/MS / Metals TCL for Waters / Water / 6020 200.8
34 / Metals – ICP/ES / Metals – TCL for Soils / Soil / 6010B 200.7
35 / Metals – ICP/MS / Metals – TCL for Soils / Soil / 6020 200.8
Costs for Chromium VI and Mercury Analyses
The determination of Chromium VI in soil requires the sample preparation procedure Method 3060A.
Task # / Task Description / Matrix / Preparation / Method / CostPer Sample
40 / Chromium VI - Color / Water / 7196A
41 / Chromium VI - Color / Soil / 3060A / 7196A
50 / Mercury - Total / Water / 7470A
245.1
51 / Mercury - Total / Soil / 7471A
52 / Mercury - Low Level / Water / 1631E
53 / Mercury - Low Level / Soil / 1631 Appendix B / 1631E
Costs to Establish Soil Fractions
The following cost applies when fine and coarse soil fractions must be established for metal analyses.
Task # / Task Description / Matrix / Method / CostPer Sample
60 / Soil Fraction / Soil / DEQ SOP #213 or Equivalent
Costs for Gasoline/Diesel Range Organics
For the below analyses, DEQ Lab parameters for extraction and carbon ranges must be used.
Task # / Task Description / Matrix / Method / CostPer Sample
100 / Gasoline Range Organics / Soil / 8015B
101 / Gasoline Range Organics / Water / 8015B
102 / Gasoline Range Organics / Water / GC/MS
103 / Gasoline Range Organics / Soil / GC/MS
104 / Diesel and Oil Range Organics / Soil / 8015B
105 / Diesel and Oil Range Organics / Water / 8015B
Organics with Laboratory TCLs
Costs for the below tasks require analyses using the professional’s TCL. The professional must provide a TCL for the analyses immediately after signing a contract.
Task # / Task Description / TCL / Matrix / Method / Cost Per Sample118 / Herbicides / Laboratory TCL / Water and Soil / 8151A
119 / Carbonyls / Laboratory TCL / Water and Soil / 8315A
120 / N-Methylcarbamates / Laboratory TCL / Water and Soil / 8318
121 / Organophosphorus Compounds / Laboratory TCL / Water and Soil / 8141A
Cost for Sampling Kit to Collect Soils Using Methanol Preservation
The cost for a methanol sampling kit applies only when not used to return a sample to the professional.
Task # / Task Description / Matrix / Method / Cost Per Sample111 / Methanol Sampling Kit / Soil / 5035A
Organics with DEQ TCLs
The costs below apply for analyses conducted for the target compound lists indicated, and included into this document.
Task # / Task Description / TCL / Matrix / Method / Cost Per Sample106 / Chlorinated Pesticides / Chlorinated Pesticides / Water/ Soil / 8081A
107 / Polychlorinated Biphenyls, Aroclors / PCBs / Water/ Soil / 8082
108 / Volatile Organic Compounds,
w TICS / Volatiles / Water/Soil / 8260B
109 / Volatile Organic Compounds,
w/o TICS / Volatiles / Water/Soil / 8260B
112 / BTEX - MTBE - & TMBs / BTEX, MTBE, TMBs / Water/Soil / 8260B
113 / Semi-volatiles Organic Compounds,
w TICS / Semivolatiles / Water/Soil / 8270C
114 / Semi-volatiles Organic Compounds, wo TICS / Semivolatiles / Water/Soil / 8270C
115 / Polynuclear Aromatic Hydrocarbons / PNAs / Water/Soil / 8270C
116 / Phenols / Phenols / Water/Soil / 8270C 8151
117 / Ethylene Dibromide and
1 - 2-Dibromo-3-chloropropane / EDB, DBCP / Water / 8260B-SIM 8011
Cost for Library Search
The cost for a library search applies when analyses conducted using Gas Chromatography with Mass Selective Detection was used but tentative identified compounds were not initially requested, or when a search for specific compounds identified by the state must be conducted.
Task # / Task Description / Method / Cost Per Sample or Report200 / Library Search / 8260B 8270C
Costs for Cyanide Analyses
Task # / Task Description / Matrix / Preparation / Method / Cost Per Sample300 / Cyanide - Total / Water / 9012A 9014 335.4
301 / Cyanide - Total (Extractable) / Soil / 9013A / 9012A 9014 335.4
302 / Cyanide - Available / Water / OIA 1677 or Equivalent
303 / Cyanide - Available (Extractable) / Soil / 9013A / OIA 1677 or Equivalent
304 / Cyanide – Total Preservation Kit / Water / Provided with Kit
305 / Cyanide Available Preservation Kit / Water / Provided With Kit
Costs to Determine Nitrogen Forms
Task # / Task Description / Matrix / Preparation / Method / Cost Per Sample400 / Ammonia / Water / 350.1 4500 NH3
401 / Ammonia / Soil / 350.1 Mod
402 / Kjeldahl Nitrogen / Water / 351.1 351.2
403 / Kjeldahl Nitrogen / Soil / 351.1 Mod.
351.2 Mod.
404 / Nitrate, Nitrite, Nitrate + Nitrite / Water / 353.2 4500 NO3 F
405 / Nitrate, Nitrite, Nitrate + Nitrite / Water / 300.0 300.1
406 / Nitrate, Nitrite, Nitrate + Nitrite / Soil / D 3987-04 / 353.2 4500 NO3 F
407 / Nitrate, Nitrite, Nitrate + Nitrite / Soil / D 3987-04 / 300.0 300.1
Costs for Organic Carbon
Task # / Task Description / Matrix / Method / Cost Per Sample500 / Total Organic Carbon (TOC) / Water / 415.1
5310C
501 / Fraction Organic Carbon / Soil / Walkley-Black
502 / Fraction Organic Carbon / Soil / Combustion
Waste Characterizations
The RCRA lists are provided in the latest guidance for waste characterization.
Task # / Task Description / TCL / Matrix / Method / Cost Per Sample600 / Ignitability - Pensky-Martens / NA / Various / 1010
601 / Ignitability - Setaflash / NA / Various / 1020A
602 / Corrosivity - Ph / NA / Various / 9040B
603 / Corrosivity - Towards Steel / NA / Various / 1110
604 / Volatile Organic Compounds / RCRA List / Extracts / 8260B
605 / Semi-volatile Organic Compounds / RCRA List / Extracts / 8270C
606 / Pesticides - RCRA / RCRA List / Extracts / 8081A
607 / Polychlorinated biphenyls, Aroclors / RCRA List / Extracts / 8082
608 / Herbicides / RCRA List / Extracts / 8151
609 / Metals / RCRA List / Extracts / Various
610 / Paint Filter Liquids Test / NA / Various / 9095
Costs for Common Environmental Parameters and Non-common Sample Extractions for Soils
700 / Alkalinity / Water / 2320 B
310.2
701 / Biochemical Oxygen Demand / Water / 5210 B
702 / Carbonaceous BOD / Water / 5210 B
703 / Chemical Oxygen Demand / Water / 410.3 410.4 5220 D
704 / Conductivity / Water / 120.1 2510 B
705 / Filtration - Dissolved Metals / Water / 3030 B
706 / Hardness - Ca-Mg Calculated / Water / 2340 B
707 / pH, Waters / Water / 9040C
4500H+B
708 / pH, Soils / Soil / 9045D
709 / Phenol / Water / 420.2 420.4 9066
710 / Solids - Total Dissolved / Water / 2540 C
711 / Solids - Total Suspended / Water / 2540 D
712 / Silica - Dissolved / Water / 200.7 3120 B 4500-Si D 4500-SiO2 C
713 / Sulfide - Total and Dissolved / Water / 4500S2- D
714 / Sulfide - Extractable / Soil / 9031 / 4500S2- D
715 / Total Solids / Water / 2540 B
716 / Turbidity / Water / 180.1
2130B
717 / TPH - Aqueous / Water / 1664
718 / TPH - Solids / Water / 9071A
719 / Chloride / Water / 4500 Cl E
720 / Chloride / Water / 300.0 300.1
721 / Chloride / Soil / D 3987-04 / 4500 Cl E
722 / Chloride / Soil / D 3987-04 / 300.0 300.1
723 / Sulfate / Water / 375.2
724 / Sulfate / Water / 300,0 300.1 ASTM 516-90(02)
725 / Sulfate / Soil / D 3987-04 / 375.2
726 / Sulfate / Soil / D 3987-04 / 300,0 300.1 ASTM 516-90(02)
727 / Fluoride / Water / 4500-F B D E
728 / Fluoride / Water / 300.0 300.1
729 / Fluoride / Soil / D 3987-04 / 4500-F B D E
730 / Fluoride / Soil / D 3987-04 / 300.0 300.1
731 / Perchlorate / Water / 314.0 or Equivalent
732 / Perchlorate / Soil / D 3987-04 / 314.0 or Equivalent
733 / Phosphorus - Total / Water / 365.4 4500P F
734 / Phosphorus - Total / Soil / 365.4 Mod
Other Services
1039 / Formaldehyde / Water / 8315
1040 / Formaldehyde / Soil / 8315
1042 / Explosives-Energetics / ExplosivesEnergetics TCL / Water or Soil / 8330
1043 / Nitroglycerin and PETN / Water or Soil / 8332
735 / Bromide / Water or Soil / 300.0 9056
736 / Total Volatile Solids / Water / 2540
122 / Chlorinated Hydrocarbons / Cl Hydrocarbons TCL / Water or Soil / 8121
123 / Acrylamide / Water or Soil / 8316
124 / Total Organic Halogens / Water / 9020B
125 / Extractable Organic Halogens / Soil / 9023
126 / Alcohols / Alcohol TCL / Water or Soil / 8015B
503 / Fraction Organic Carbon / Soil / D2974-87
737 / Color / Water / NCASI 71.01
3000 / Acidic Acid / Water or Soil / EPA 8015
3001 / Carbon Dioxide / Water / SM 4500
3002 / Gases, Dissolved / Water or Air / ISOTECH
3003 / Grain Size / Soil / ASTM D421/422
3004 / Herbicides, Total / Water or Soil / EPA 8151
3005 / Iron, Ferrous / Water / SM 3500
3006 / Mercury, Total / Waste Water / EPA 245.1
3007 / Methane / Water or Air / ISOTECH
1041 / Dissolved Gases
Methane/Ethane/
Ethene / Methane/Ethane/
Ethene / Water or Air / RSK 175
3008 / Dissolved Gases
Methane/Ethane/
Ethene / Methane/Ethane/
Ethene / Water or Air / ISOTECH
3009 / Method 24 / Paints / EPA 24
3010 / Reactive Cyanide / Water or Soil / SW 846
3011 / Reactive Sulfide / Water or Soil / SW 846
3012 / Surfactants (MBA’s) / Water / SW5540
3013 / TOX / Oil / EPA 9076
3014 / EOX / Soil / EPA 9023
3015 / VOC’s / Air / EPA 8260
3016 / VOC’s / Air-tedlar / TO-15
3017 / VOC’s / Air-bottle vac / TO-15
3018 / VOC’s / Air-canister / TO-15
3019 / VOC / Fatty Acid (1) / EPA 8015
3020 / VOC / Fatty Acid (3) / EPA 8015
3021 / VOC Exempt from method 24 / Paints / EPA 8260
3022 / Glycol / Water or Soil / EPA 8015
127 / Pesticides Specialty Chemistry List / Pesticide Specialty Chemistry List TCL / Water or Soil / 8081A
Incremental Sampling Method (IMS)
Task # / Task Description / Matrix / Preparation / Cost Per Sample
4001 / ISM Processing-1Kg (Dry, Disaggregate, #4 or #10 Sieve, 2-D Subsample 1 method) / Soil / Non-volatile Analysis
4002 / ISM Processing - each additional Kg / Non-volatile Analysis
4003 / 2-Dimensional Slabcake subsampling-each additional analyte fraction / Soil / Non-volatile Analysis
4004 / Particle size determination (additional sleving or wet sieving) / Soil / Non-volatile Analysis
4005 / Puck Mill - each Kg / Soil / Non-volatile Analysis
4006 / Ball Mill - each Kg / Soil / Non-volatile Analysis
4007 / 3 gran Mercury prep / Soil / Non-volatile Analysis
4008 / 10 gran Metals prep / Soil / Non-volatile Analysis
4009 / 1L narrow mouth bottle with 300mls MeOH for 30 increments / Soil / Volatile Analysis
4010 / 1L narrow mouth bottle with 500 mls MeOH for 50 increments / Soil / Volatile Analysis
4011 / 2 L narrow mouth bottle with 1000mls MeOh for 100 increments / Soil / Volatile Analysis
4012 / 1 L narrow mouth bottle with 300mls MeOh for 30 increments (MS/MSD) 2 bottles needed / Soil / Volatile Analysis
4013 / 1 L narrow mouth bottle with 500mls MeOh for 50 increments (MS/MSD) 2 bottles needed / Soil / Volatile Analysis
4014 / 2 L narrow mouth bottle with 1000mls MeOh for 100 increments (MS/MSD) 2 bottles needed / Soil / Volatile Analysis
4015 / 40ml vial with 10ml MeOH (1 vial per increment) / Soil / Volatile Analysis
Cost Table
Costs for Premiums
Task # / Task Description / Multiplier800 / Premium, 24 hour
801 / Premium, 2-3 day
802 / Premium, 4-7 day
803 / Premium, 8-13 day
POSITION, CLASSIFICATION AND EMPLOYEE BILLING RATE INFORMATION