UCSF Lab Standard Operating Procedure

Chemical Process, Name or Hazard Class:

Methylazoxymethanol Acetate

Please fill out the form completely.

Insure all users have access to this SOP.

Refer to instructions for assistance.

Department: / Enter text.
Date SOP was written: / Enter date.
This lab specific SOP has been reviewed and approved by:
Principal Investigator Name: / Enter text.
Principal Investigator Signature
Lab Manager/Supervisor: / Enter text.

Type of SOP: ☐ Process ☒Hazardous Chemical ☐ Hazardous Class

Purpose

Methylazoxymethanol acetate is a combustible liquid. It is toxic if ingested and may be harmful if inhaled or absorbed through the skin. It is corrosive to skin, eyes, mucous membranes, and upper respiratory tract. It is classified by IARC as Group 2B, possibly carcinogenic to humans. It is a suspected reproductive toxicant. Methylazoxymethanol acetate is a potent alkylating agent and neurotoxin used for research purposes. It is found in cycad leaves and seeds.

Physical & Chemical Properties/Definition of Chemical Group

CAS#: 592-62-1

Class: Combustible, toxic, corrosive, carcinogen, reproductive toxin

Molecular Formula: C4H8N2O3

Form (physical state): Liquid

Color: Colorless

Boiling point: 191 °C

Potential Hazards/Toxicity

Methylazoxymethanol acetate is a combustible liquid. It is toxic if ingested and may be harmful if inhaled or absorbed through the skin. It may cause irritation to the gastrointestinal tract, respiratory tract, skin, and eyes. It is corrosive to skin, eyes, mucous membranes, and upper respiratory tract. It is classified by IARC as Group 2B, possibly carcinogenic to humans. It may cause harm to the unborn child. Symptoms of exposure include nausea, vomiting, headache, dizziness, tiredness, erythema, pneumonitis, pulmonary edema, and unconsciousness.

Engineering Controls

Chemical fume hood. Adequate exhaust and capture filtration. Electrically grounded lines and equipment.

Personal Protective Equipment (PPE)

Respirator Protection

If lab personnel would like to use respirator on a voluntary basis, they must be trained and fit-tested by EH&S. This is a regulatory requirement. (http://or.ucsf.edu/ehs/8193-DSY/version/default/part/4/data/)

Hand Protection

Handle with gloves. Nitrile gloves are recommended.

NOTE: Consult with your preferred glove manufacturer to ensure that the gloves you plan on using are compatible with methylazoxymethanol acetate.

Refer to glove selection chart from the links below:

http://www.ansellpro.com/download/Ansell_8thEditionChemicalResistanceGuide.pdf

OR

http://www.allsafetyproducts.biz/page/74172

OR

http://www.showabestglove.com/site/default.aspx

OR

http://www.mapaglove.com/

Eye Protection

ANSI approved, tight-fitting glasses/goggles. Face shields are recommended.

Skin and Body Protection

Flame-resistant lab coat preferably made of antistatic material, long pants, closed-toe shoes.

Hygiene Measures

Avoid contact with skin, eyes, and clothing. Wash hands before breaks and after handling.

First Aid Procedures

If inhaled

Move person into fresh air. If not breathing, give artificial respiration. If breathing is difficult, give oxygen. Consult a physician.

In case of skin contact

Immediately flush with plenty of water for at least 15 minutes while removing contaminated clothing. Consult a physician. Take victim immediately to the hospital.

In case of eye contact

Flush eyes with plenty of water for at least 15 minutes lifting upper and lower eyelids and removing contact lenses. Consult a physician. Continue rinsing eyes during transport to the hospital.

If swallowed

Do not induce vomiting. Never give anything by mouth to an unconscious person. If victim is conscious and alert, rinse mouth with water. Consult a physician.

Special Handling and Storage Requirements

Precautions for safe handling: Avoid contact with skin, eyes, and clothing. Avoid inhalation and ingestion. Use spark-proof tools and explosion-proof equipment. Provide adequate ventilation. Keep away from heat and other sources of ignition- No smoking. Prevent build-up of electrostatic charge.

Conditions for safe storage: Keep container tightly closed in a cool, dry, and well-ventilated area. Opened containers must be carefully resealed and kept upright to prevent leakage. Recommended storage temperature is 4 °C. Avoid strong oxidizing agents, strong acids, and strong bases.

Spill and Accident Procedure

Chemical Spill Dial 9-911 from campus phone or 415-476-1414 from cell phone or 415-206-8522 (SFGH only)

Spill – Assess the extent of danger. Assist contaminated or injured persons. Evacuate the spill area. Avoid breathing vapors. If possible, confine the spill to a small area using a spill kit or absorbent material. Keep others from entering contaminated area (e.g., use caution tape, barriers, etc.).

Small (<1 L) – If you have training, you may assist in the clean-up effort. Use appropriate personal protective equipment and clean-up material for chemical spilled. Double bag spill waste in clear plastic bags, label and take to the next chemical waste pick-up.

Large (>1 L) – Dial 9-911 from campus phone or 415-476-1414 from cell phone or 415-206-8522 (SFGH only) for assistance.

Chemical Spill on Body or Clothes – Remove clothing and rinse body thoroughly in emergency shower for at least 15 minutes. If discomfort persists, proceed to the Emergency Department. If no further discomfort is experienced, have the SDS ready and contact Poison Control Hotline at 1-800-222-1222 for further exposure information. Notify your direct supervisor and EH&S at 415-476-1300 during work hours, or 9-911 during non-working hours and weekends.

Chemical Splash Into Eyes – Immediately rinse eyeball and inner surface of eyelid with water for 15 minutes by forcibly holding the eye open. If discomfort persists, proceed to the Emergency Department. If no further discomfort is experienced, have the SDS ready and contact Poison Control Hotline at 1-800-222-1222 for further exposure information. Notify your direct supervisor and EH&S at 415-476-1300 during work hours, or 9-911 during non-working hours and weekends.

Medical Emergency Dial 9-911 (campus phone) or 476-6911 (cell phone)

Note: All serious injuries must be reported to EH&S at 415-476-1300 within 8 hours.

Non-Life Threatening Emergency– Go to Occupational Health Programs (OHP) Clinic, 415-885-7580, 2330 Post Street, Suite 460 Hours of Operation for Appointments: Monday - Friday 7:30 a.m. - 4:00 p.m. (except Holidays).

Note: All serious injuries must be reported to EH&S at 415-476-1300 within 8 hours.

Needle stick/puncture exposure (as applicable to chemical handling procedure) – Wash the affected area with antiseptic soap and warm water for 15 minutes. For mucous membrane exposure, flush the affected area for 15 minutes using an eyewash station. Page the needle stick nurse by dialing 415-353-7842 (STIC).

Decontamination/Waste Disposal Procedure

Clean contaminated surfaces with soap and water and paper towels. Dispose of the paper towels as hazardous waste.

Safety Data Sheet (SDS) Location

Online SDS can be accessed at http://or.ucsf.edu/ehs/7241-DSY/msds.html

Protocol/Procedure

Quantities covered by this SOP:

______(g , ml) to ______(g, ml)

Temperature range covered by this SOP:

__ °C – __ °C

General Overview and Purpose:

Enter the experimental purpose

Procedure:

Enter experimental procedure. You can copy procedure from your lab notebook or from literature.

NOTE

Any deviation from this SOP requires approval from the Principal Investigator.

Methylazoxymethanol Acetate 4 Date: Click here to enter a date.

Modified from SOP templates developed by UCLA EH&S (http://www.sop.ehs.ucla.edu/)