Summary of Epa Emission Test Methods

January 19, 2019

SUMMARY OF EPA EMISSION TEST METHODS

Title 40

Office of Air Quality Planning and Standards

Method Reference Description

Part 51, Appendix M

20155 FR 1424604/17/90 PM-10 (EGR procedure).

201A55 FR 1424604/17/90 PM-10 (CSR procedure).

201A 55 FR 2468706/18/90Correction of equations.

20155 FR 3760609/12/90Correction of equations.

20256 FR 6543312/17/91Condensible PM.

203P57 FR 4611410/07/92COMS QA for compliance.(See Part 60, App F, Proc 3)

203A P58 FR 6164011/22/93Visible Emissions - 2-6 min avg.

203B P58 FR 6164011/22/93Visible Emissions - time exceptions.

203C P58 FR 6164011/22/93Visible Emissions - instantaneous.

20462 FR 3250006/16/97VOC Capture Efficiency.

204A 62 FR 3250006/16/97VOC Capture Efficiency.

204B 62 FR 3250006/16/97VOC Capture Efficiency.

204C 62 FR 3250006/16/97VOC Capture Efficiency.

204D 62 FR 3250006/16/97VOC Capture Efficiency.

204E 62 FR 3250006/16/97VOC Capture Efficiency.

204F62 FR 3250006/16/97VOC Capture Efficiency.

20559 FR 1959005/30/94Dilution calibration verification.

206(Now CTM-027)Ammonia (NH3)

207P62 FR 6453212/08/97Isocyanates.

Part 60, Appendix A

1-842 FR 41754 08/18/77Velocity, Orsat, PM, SO2, NOx, etc.

43 FR 1198403/23/78Corr. and amend. to M-1 thru 8.

1-24 52 FR 3463909/14/87Technical corrections.

52 FR 4206111/02/87Corrections.

2-2555 FR 4747111/14/90Technical amendments.

1-29P62 FR 4563908/27/97Reformat and revise methods.

1-2965 FR 61744 10/17/02Performance specs.

148 FR 4503409/30/83Reduction of number of traverse points.

151 FR 2028606/04/86Alternative procedure for site selection.

1A54 FR 1262103/28/89Traverse points in small ducts.

2A48 FR 3759208/18/83Flow rate in small ducts - vol. meters.

2B48 FR 3759408/18/83Flow rate - stoichiometry.

2C54 FR 1262103/28/89Flow rate in small ducts - std. pitot.

2D54 FR 1262103/28/89Flow rate in small ducts - rate meters.

2E61 FR 992903/12/96Flow rate from landfill wells.

2F64 FR 2648405/14/993D pitot for velocity.

2G64 FR 2648405/14/992D pitot for velocity.

2H64 FR 2648405/14/99Velocity decay near the stack wall.

355 FR 0521102/14/90 Molecular weight.

3/3B 55 FR 1887605/07/90Method 3B applicability.

3A51 FR 2116406/11/86Instrumental method for 02 and CO2.

3B55 FR 0521102/14/90 Orsat for correction factors and excess air.

3C61 FR 992903/12/96Gas composition from landfill gases.

348 FR 4945810/25/83Addition of QA/QC.

448 FR 5567012/14/83 Addition of QA/QC.

548 FR 5567012/14/83Addition of QA/QC.

545 FR 6675210/07/80Filter specification change.

548 FR 3901008/26/83DGM revision.

550 FR 0116401/09/85Incorp. DGM and probe cal. procedures.

552 FR 0965703/26/87Use of critical orifices as cal stds.

552 FR 2288806/16/87Corrections.

5A47 FR 3413708/06/82PM from asphalt roofing (Prop. as M-26).

5A51 FR 3245409/12/86Addition of QA/QC.

5B51 FR 4283911/26/86Nonsulfuric acid PM.

5CTentativePM from small ducts.

5D49 FR 4384710/31/84PM from fabric filters.

5D51 FR 3245409/12/86Addition of QA/QC.

5E50 FR 0770102/25/85PM from fiberglass plants.

5F51 FR 4283911/26/86PM from FCCU.

5F53 FR 2968108/08/88Barium titration procedure.

5G53 FR 0586002/26/88PM from wood stove - dilution tunnel.

5H53 FR 0586002/26/88PM from wood stove - stack.

5I64 FR 5302709/30/99PM for RATA of PM CEMS.

649 FR 2652206/27/84Addition of QA/QC.

648 FR 3901008/26/83DGM revision.

652 FR 4142310/28/87Use of critical orifices for FR/vol meas.

6A47 FR 5407312/01/82SO2/CO2 - manual method.

6B47 FR 5407312/01/82Auto SO2/CO2.

6A/B49 FR 0968403/14/84Incorp. coll. test changes.

6A/B51 FR 3245409/12/86Addition of QA/QC.

6C51 FR 2116406/11/86Instrumental method for S02.

6C52 FR 1879705/27/87Corrections.

749 FR 2652206/27/84Addition of QA/QC.

7A48 FR 5507212/08/83Ion chromatograph NOx analysis.

7A53 FR 2013906/02/88ANPRM.

7A55 FR 2175205/29/90 Revisions.

7B50 FR 1589304/23/85UV N0x analysis for nitric acid plants.

7A/BTentativeHigh SO2 interference.

7C49 FR 3823209/27/84Alkaline permanganate/colorimetric for NOx.

7D49 FR 3823209/27/84Alkaline permanganate/IC for NOx.

7E51 FR 2116406/11/86Instrumental method for NOx.

836 FR 2487612/23/71Sulfuric Acid mist and SO2.

842 FR 4175408/18/77Addition of particulate and moisture.

8 43 FR 11984 03/23/78Miscellaneous corrections

939 FR 3987211/12/74Opacity.

9A46 FR 5314410/28/81Lidar opacity; called Alternative 1.

1039 FR 0931903/08/78CO.

1053 FR 4133310/21/88Alternative trap.

10A52 FR 3067408/17/87Colorimetric method for PS-4.

10A52 FR 3331609/02/87Correction notice.

10B53 FR 4133310/21/88GC method for PS-4.

1143 FR 0149401/10/78H2S.

1247 FR 1656404/16/82Pb.

1249 FR 3384208/24/84Incorp. method of additions.

13A45 FR 4185206/20/80F - colorimetric method.

13B45 FR 4185206/20/80F - SIE method.

13A/B45 FR 8501612/24/80Corr. to M-13A and 13B.

1445 FR 4420206/30/80F from roof monitors.

14A62 FR 52383 10/07/97F from roof monitors- Alcan cassettes.

1543 FR 1086603/15/78TRS from petroleum refineries.

1554 FR 4623611/02/89Revisions.

1554 FR 5155012/15/89Correction notice.

15A52 FR 2039106/01/87TRS alternative/oxidation.

1643 FR 0756802/23/78TRS from kraft pulp mills.

1643 FR 3478408/07/78Amend. to M-16, H2S loss after filters.

1644 FR 0257801/12/79Amend. to M-16, S02 scrubber added.

1654 FR 4623611/02/89Revisions.

1655 FR 2175205/29/90Correction of figure (10%).

16A50 FR 0957803/08/85TRS alternative.

16A52 FR 3640809/29/87Cylinder gas analysis alternative method.

16B52 FR 3640809/29/87TRS alternative/GC analysis of S02.

16A/B53 FR 0291402/02/88Correction 16A/B.

1743 FR 0756802/23/78PM, in-stack.

1848 FR 4834410/18/83VOC, general GC method.

18 49 FR 2260805/30/84Corrections to M-18.

1852 FR 5110502/19/87Revisions to improve method.

1852 FR 1085204/03/87Corrections.

1859 FR 1930804/22/94Revisions to improve QA/QC.

1944 FR 3358006/11/79F-factor, coal sampling.

1952 FR 4782612/16/87M-19A incorp, into M-19

1948 FR 4946010/25/83Corr. to F factor equations and Fc value.

2044 FR 5279209/10/79NOx from gas turbines.

2047 FR 3048007/14/82Corr. and amend.

2051 FR 3245409/12/86Clarifications.

2148 FR 3759808/18/83VOC leaks.

2149 FR 5658012/22/83Corrections to Method 21.

2155 FR 2560206/22/90Clarifying revisions.

2247 FR 3413708/06/82Fugitive VE.

2248 FR 4836010/18/83Add smoke emission from flares.

2356 FR 575802/13/91 Dioxin/dibenzo furan.

23 P60 FR 2837805/31/95Revisions and corrections.

2445 FR 6595610/03/80Solvent in surface coatings.

24A47 FR 5064411/08/82Solvent in ink (Prop. as M-29).

24TentativeSolvent in water-borne coatings.

2457 FR 3065407/10/92Multicomponent coatings.

2460 FR 4709509/11/95Radiation-cured coatings.

2545 FR 6595610/03/80TGNMO.

2553 FR 0414002/12/88Revisions to improve method.

2553 FR 1159004/07/88Correction notice.

25A48 FR 3759508/18/83TOC/FID.

25B48 FR 3759708/18/83TOC/NDIR.

25C61 FR 992903/12/96VOC from landfills.

25D59 FR 1931104/22/94VO from TSDF - purge procedure.

25E59 FR 6289612/06/94VO from TSDF - vapor pressure procedure.

2656 FR 575802/13/91 HCl.

2657 FR 2455006/10/92Corrections to Method 26.

2659 FR 1930904/22/94Add 26 HCl, halogens, other hydrogen halides.

26A59 FR 1930904/22/94Isokinetic HCl, halogens, hydrogen halides.

2748 FR 3759708/18/83Tank truck leaks.

2853 FR 0586002/26/88Wood stove certification.

28A53 FR 0586002/26/88Air to fuel ratio.

2961 FR 1826204/25/96Multiple metals.

2963 FR 0649302/09/98Amends promulgation dates.

Part 60, Appendix B

PS-2 - 9 P62 FR 4563908/27/97Reformat and revise performance specs.

PS-2 - 965 FR 61744 10/17/02Reformat and revise performance specs.

PS-148 FR 1332203/30/83Opacity.

PS-1P59 FR 6058511/25/94Revisions.

PS-165 FR 4891408/10/00Revisions, final rule.

PS-248 FR 2360805/25/83SO2 and NOx.

PS 1-555 FR 4747111/14/91Technical amendments.

PS-348 FR 2360805/25/83CO2 and O2.

PS-450 FR 3170008/05/85CO.

PS-4A56 FR 552602/11/91CO for MWC.

PS-4B P61 FR 1749504/19/96CO and O2 for HWI (BIF rules)

PS-4B64 FR 5303209/30/99Final rule.

PS-548 FR 3298407/20/83TRS.

PS-653 FR 0751403/09/88Velocity and mass emission rate.

PS-755 FR 4017110/02/90 H2S.

PS-859 FR 6458012/15/94VOC CEMS performance specifications.

PS-8A P61 FR 1749504/19/96VOC CEMS for HWI (BIF rules)

PS-8A64 FR 5303309/30/99Final rule.

PS-9 59 FR 6458012/15/94GC CEMS performance specifications.

PS-10 P61 FR 1749504/19/96Metals CEMS(HWC MACT)

PS-1169 FR 178601/12/04PM CEMS.

PS-11A P61 FR 1749504/19/96PM CEMS (HWC MACT).

PS-12A70 FR 2860605/18/05Hg CEMS(Coal-fired Boilers)

PS-12 P61 FR 1749504/19/96Hg CEMS (HWC MACT).

PS-13 P61 FR 1749504/19/96HCl CEMS (HWC MACT).

PS-14 P61 FR 1749504/19/96Cl CEMS (HWC MACT).

PS-15 P62 FR 4537208/27/97FTIR CEMS.

PS-16 P 70 FR 45608 08/08/05Predicative Emissions Monitoring Systems

Part 60, Appendix F

Proc 152 FR 2100306/04/87Quality assurance for CEMS.

Proc 156 FR 552702/11/91 Revision.

Proc 269 FR 1768 01/12/04QA for PM CEMS

Proc 3 P 68 FR 24692 05/08/03QA for COMS

Part 60, Appendix J

App-J55 FR 3392508/20/90Wood stove thermal efficiency.

Alternative Procedures and Miscellaneous

48 FR 4470009/29/83S-Factor method for sulfuric acid plants.

48 FR 4866910/20/83Corrections to S-Factor publication.

49 FR 3067207/31/84Add fuel analysis procedures for gas turbines.

51 FR 2176206/16/86Alternative PST for low level concentrations.

54 FR 4623411/02/89 Misc. revisions to Appendix A, 40 CFR Part 60.

55 FR 4017110/02/90 Monitoring revisions to Subpart J (Petr. Ref.).

Part 60

54 FR 0666002/14/89Test methods & procedures rev. (40 CFR 60).

54 FR 2134405/17/89Correction notice.

54 FR 2701506/27/89Correction notice.

Part 61, Appendix B

101-111 P62 FR 4563908/27/97Reformat, revise, amend methods.

10147 FR 2470306/08/82Hg in air streams.

101A47 FR 2470306/08/82Hg in sewage sludge incinerators.

101A61 FR 1826204/25/96Revisions - Consistency with Method 29.

10149 FR 3576809/12/84Corrections to M-101 and 101A.

10247 FR 2470306/08/82Hg in H2 streams.

10348 FR 5526612/09/83Revised Be screening method.

10448 FR 5526812/09/83Revised beryllium method.

10540 FR 4829910/14/75Hg in sewage sludge.

10549 FR 3576809/12/84Revised Hg in sewage sludge.

10647 FR 3916809/07/82Vinyl chloride.

10747 FR 3916809/07/82VC in process streams.

10752 FR 2039706/01/87Alternative calibration procedure.

107A47 FR 3948509/08/82VC in process streams.

10851 FR 2803508/04/86Inorganic arsenic.

108A51 FR 2803508/04/86Arsenic in ore samples.

108B51 FR 2202605/31/90Arsenic in ore alternative.

108C55 FR 2202605/31/90Arsenic in ore alternative.

108B/C55 FR 3291308/13/90Correction notice.

11150 FR 0519702/06/85Polonium-210.

11454 FR 5169512/15/89Monitoring of radio nuclides.

11554 FR 5170212/15/89Radon-222.

Part 61

53 FR 3697209/23/88Corrections.

Part 63 Appendix A

303-306 P62 FR 4563908/27/97Reformat and revise methods.

303-30665 FR 61744 10/17/02 Reformat and revise methods.

30157 FR 6197012/29/92Field data validation protocol.

301 P 69 FR 76642 12/22/04Revisions

302(Reserved)

30358 FR 5789810/27/93Coke Oven Door Emissions.

304A62 FR 279301/17/97Biodegradation rate (vented).

304B62 FR 279301/17/97Biodegradation rate (enclosed).

30559 FR 1959004/22/94Compound specific liquid waste.

30660 FR 494801/25/95Chromium from electroplaters/anodizers.

306A60 FR 494801/25/95Simplified Chromium sampling.

306B60 FR 4948 01/25/95Surface tension of chromium suppressors.

30759 FR 6180112/02/94Solvent Degreaser VOC.

308 P 58 FR 66079 12/17/93Methanol

30863 FR 1850404/15/98Methanol (Pulp and Paper MACT I )

309P59 FR 2921606/04./94Aerospace solvent recovery material balance.

310A62 FR 1254603/17/97Residual hexane in EPDM rubber.

310B62 FR 1254603/17/97Residual hexane in EPDM rubber.

310C62 FR 1254603/17/97Residual hexane in EPDM rubber.

311 60 FR 6293012/07/95VOC HAPS in furniture coatings.

312A62 FR 1254603/17/97Residual styrene in SBR rubber.

312B62 FR 1254603/17/97Residual styrene in SBR rubber.

312C62 FR 1254603/17/97Residual styrene in SBR rubber.

313A62 FR 1254603/17/97Residual styrene in PBR rubber.

313B62 FR 1254603/17/97Residual styrene in PBR rubber.

314TentativeHalogentated compounds in solvents.

31562 FR 5241810/07/97 MeCl Extractable organic matter.

316P62 FR 1525703/31/97Formaldehyde - manual method.

317TentativePhenol - manual method.

318P62 FR 5226603/31/97Formaldehyde, phenol, methanol with FTIR.

319 P61 FR 55862 10/29/96Filter efficiency; paint over-spray

31963 FR 4652503/27/98Filter efficiency, paint over-spray.

32064 FR 3189806/14/99Extractive FTIR.

32164 FR 3189806/14/99FTIR for HCl from Portland Cement kilns.

322P63 FR 14244 03/24/98GFC/IR for HCl from Portland cement kilns.

323 P 68 FR 1925 01/14/03Formaldehyde from Natural Gas-Fired sources.

P = Proposal

Tentative = Under evaluation